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This volume of "Inorganic Syntheses" spans the preparations of wide range of important inorganic, organometallic and solid-state compounds. The volume is divided into 6 chapters. The first chapter contains the syntheses ofsome key early transition metal halide clusters and the very useful mononuclear molybdenum(III) synthon, MoCl3(THF)3. Chapter 2 covers the synthesis of a number of cyclopentadienyl compounds, including a novel route to sodium and potassium cyclopentadienide, MC5H5. Chapter 3 details synthetic procedures for a range of metal-metal bonded compounds, including several with metal-metal multiple bonds. Chapter 4 contains procedures for a range ofearly and late transition metal compounds, each a useful synthon for further synthetic elaboration. Chapter 5 dealswith the synthesis of a number of main group compounds and ligands, while Chapter 6 covers teaching laboratory experiments.